Web28.3 Step 3: Preparation of 5,6-dimethoxyisobenzofuran-1,3-dione (154) A suspension of 4,5-dimethoxyphthalic acid (600 mg, 2.65 mmol) in acetic anhydride (5 ml) was heated to 120° C. for 1 hour. The solvent was then removed under vacuum to afford 5,6-dimethoxyisobenzofuran-1,3-dione as a yellow solid (552 mg, 2.65 mmol, quantitative yield). WebBiotage® MP-TsOH resin is a sulfonated macroporous polystyrene resin and has been optimized for use as a bound reagent or scavenger resin for the synthesis of small molecules. The sulfonic acid groups in MP-TsOH are readily accessible for removal of basic compounds (e.g. primary, secondary, and tertiary amines) by quaternary salt formation.
p-Toluenesulfonic acid - Wikipedia
WebSep 13, 2024 · What is TsOH organic chemistry? Toluenesulfonic acid (p-toluenesulfonic acid; TsOH; p-TsOH): An aromatic sulfonic acid, often used as a strong acid catalyst. … WebThe saline used in our experiments had a pH value of 5.15. On the other side, the carboxypentyl group in Cy7COOH and ICy7COOH as well as propanesulfonate group in ICy7SO 3 H are more acidic (e.g ... bishop auckland food festival 2021
Reactions of Esters: Explanation, Examples & Formation
WebMar 3, 2024 · The study commenced by investigating suitable conditions for the synthesis of diaryliodonium salts 3 from the corresponding ortho-iodoazobenzenes 1. 24 Our standard one-pot conditions with m CPBA and triflic or tosic acid and a suitable arene failed, 23b,d as did one-pot reactions of 1 with arylboronic acids. 23c To our delight, a sequential one-pot … http://www.chem.ucla.edu/~harding/IGOC/T/toluenesulfonic_acid.html WebActivated steel (AC) equipped a very highs surface area of over 2000 m2/g was produced from base sulfur acid hydrotropic lignin (AHL) from poplar wood by H3PO4 at a modest temperature of 450 °C (AHL-AC6). ACs by similar surface areas were also obtained under the same activation condition from commercial hardwood alkali lignin and … bishop auckland food bank